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Originally Posted by dirtwarrior

I need a step by step or a youtube video on how to do the syringe filter.
Thanks

Do this going that route.

Get 60ml Termo syringe
Get millipore syringe filter cause it's bigger volume at time or use what floats your boat.

Get caulk gun.
Get 50ml sterile vial or bigger.
In caulk gun Termo syringe filter can be filled with 47ml at time to fit inside.
Get a rod and big fat rubber bands
Use them to hold rod around caulk gun and vial to rod to hang below.

Use a 20ga needle attached to filter going into vial and a 20ga or 20 ga to use as vent vial while filling with syringe filter.
I used 21ga with 23ga vent before.


Get your gear.
Weight it out. Look up standard recipes and follow say for 50ml at time of whatever.
Use 15% BB
And 2% BA
So get weight of raw, volume quantity, and calculate or use proven recipe.

Put desired amount of powder into glass beaker.
Add proper amounts of bb and ba.
I put on stove I get a skillet put an inch of water and turn on medium and out beaker in middle. I adjust heat accordingly.
I only heat until completely clear.
I never have checked temp.

At same time I put measured amount of carrier oil in seperate beaker in oven at 200 degrees for around 20 minutes.

I remove add both together and put into oven at around 200 degrees for a few minutes.
I never let get hotter than 150-170 degrees.
That I measure with cooking thermometer inside of empty vial on surface.
MAKE NO CONTACT WITH ANYTHING METAL!!!

I let cool to around 120 degrees and filter thru bottle top with vac pump or syringe filter.

Here us photo if syringe filter caulk set up.
U crank a little now and then, no pain on finger. Rig 2 or 3 at time if u like.
Hang caulk gun in a cabinet or whatever.

This route it stays sterile going into sterile vial. U can always put into 10ml vials and can change rubber and recrimp new safety top. Soak rubber in 70% alcohol let dry change out. Also I dip metal top crimpable piece in alcohol and wipe.

I have done this route and it's easy.
I do same with bottle top zap cap and media bottle. I only sterilize media bottle and I draw out with pipette to fill vials then crimp with sterile rubber of course.
Instead of sterilizing vials I buy sterile and remove metal crimped piece remove rubber replace with new sterilized rubber I soak dry put on then crimp.

I have done this for personal use only in past. So top not important to have safety top but I just told u how that is changed to have.
Crimp tool?? Lol!!
A butter knife bending around with pressure pushing on tip with finger no one can tell. I have other things I made as easier cheap crimp tool.

Hope this helped u.

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Originally Posted by Musclemechanic76

Do this going that route.

Get 60ml Termo syringe
Get millipore syringe filter cause it's bigger volume at time or use what floats your boat.

Get caulk gun.
Get 50ml sterile vial or bigger.
In caulk gun Termo syringe filter can be filled with 47ml at time to fit inside.
Get a rod and big fat rubber bands
Use them to hold rod around caulk gun and vial to rod to hang below.

Use a 20ga needle attached to filter going into vial and a 20ga or 20 ga to use as vent vial while filling with syringe filter.
I used 21ga with 23ga vent before.


Get your gear.
Weight it out. Look up standard recipes and follow say for 50ml at time of whatever.
Use 15% BB
And 2% BA
So get weight of raw, volume quantity, and calculate or use proven recipe.

Put desired amount of powder into glass beaker.
Add proper amounts of bb and ba.
I put on stove I get a skillet put an inch of water and turn on medium and out beaker in middle. I adjust heat accordingly.
I only heat until completely clear.
I never have checked temp.

At same time I put measured amount of carrier oil in seperate beaker in oven at 200 degrees for around 20 minutes.

I remove add both together and put into oven at around 200 degrees for a few minutes.
I never let get hotter than 150-170 degrees.
That I measure with cooking thermometer inside of empty vial on surface.
MAKE NO CONTACT WITH ANYTHING METAL!!!

I let cool to around 120 degrees and filter thru bottle top with vac pump or syringe filter.

Here us photo if syringe filter caulk set up.
U crank a little now and then, no pain on finger. Rig 2 or 3 at time if u like.
Hang caulk gun in a cabinet or whatever.

This route it stays sterile going into sterile vial. U can always put into 10ml vials and can change rubber and recrimp new safety top. Soak rubber in 70% alcohol let dry change out. Also I dip metal top crimpable piece in alcohol and wipe.

I have done this route and it's easy.
I do same with bottle top zap cap and media bottle. I only sterilize media bottle and I draw out with pipette to fill vials then crimp with sterile rubber of course.
Instead of sterilizing vials I buy sterile and remove metal crimped piece remove rubber replace with new sterilized rubber I soak dry put on then crimp.

I have done this for personal use only in past. So top not important to have safety top but I just told u how that is changed to have.
Crimp tool?? Lol!!
A butter knife bending around with pressure pushing on tip with finger no one can tell. I have other things I made as easier cheap crimp tool.

Hope this helped u.

Sent from my SAMSUNG-SM-G890A using Tapatalk

Supplies needed.
- Termo 60ml syringe
- sterile needles to connect to filter and to vent vial 20ga to 23ga
Syringe filters.
- I personally use .45um with syringe route never had an issue ever!!
Used .22um in caulk gun too.
- a brand new clean caulk gun. Wipe with alcohol pads.
- box of alcohol pads
- pack of cotton pads
- 70% alcohol and 90% too
- 2 glass beakers
- dial soap to wash beaker
- distilled water to rinse after washing.
- spray bottles to spray with distilled water then alcohol to clean beakers. I do this even though it's being filtered from beaker.
- 50ml sterile vials or bigger.
- BB (benzoylbenzate)
- BA ( benzoyl Alcohol)
- carrier oil GSO, MCT, Cottonseed, etc etc.......
-sterile gloves latex or whatever I get a pack or box
- preferably a glass thermometer for liquids
- a digital scale that can weight point whatever of a gram sensitivety.
- a nickel 5 grams to celebrate scale
-rubber bands or zip ties whatever u choose to hold it.

That is about it!!



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Originally Posted by Musclemechanic76

Do this going that route.

Get 60ml Termo syringe
Get millipore syringe filter cause it's bigger volume at time or use what floats your boat.

Get caulk gun.
Get 50ml sterile vial or bigger.
In caulk gun Termo syringe filter can be filled with 47ml at time to fit inside.
Get a rod and big fat rubber bands
Use them to hold rod around caulk gun and vial to rod to hang below.

Use a 20ga needle attached to filter going into vial and a 20ga or 20 ga to use as vent vial while filling with syringe filter.
I used 21ga with 23ga vent before.


Get your gear.
Weight it out. Look up standard recipes and follow say for 50ml at time of whatever.
Use 15% BB
And 2% BA
So get weight of raw, volume quantity, and calculate or use proven recipe.

Put desired amount of powder into glass beaker.
Add proper amounts of bb and ba.
I put on stove I get a skillet put an inch of water and turn on medium and out beaker in middle. I adjust heat accordingly.
I only heat until completely clear.
I never have checked temp.

At same time I put measured amount of carrier oil in seperate beaker in oven at 200 degrees for around 20 minutes.

I remove add both together and put into oven at around 200 degrees for a few minutes.
I never let get hotter than 150-170 degrees.
That I measure with cooking thermometer inside of empty vial on surface.
MAKE NO CONTACT WITH ANYTHING METAL!!!

I let cool to around 120 degrees and filter thru bottle top with vac pump or syringe filter.

Here us photo if syringe filter caulk set up.
U crank a little now and then, no pain on finger. Rig 2 or 3 at time if u like.
Hang caulk gun in a cabinet or whatever.

This route it stays sterile going into sterile vial. U can always put into 10ml vials and can change rubber and recrimp new safety top. Soak rubber in 70% alcohol let dry change out. Also I dip metal top crimpable piece in alcohol and wipe.

I have done this route and it's easy.
I do same with bottle top zap cap and media bottle. I only sterilize media bottle and I draw out with pipette to fill vials then crimp with sterile rubber of course.
Instead of sterilizing vials I buy sterile and remove metal crimped piece remove rubber replace with new sterilized rubber I soak dry put on then crimp.

I have done this for personal use only in past. So top not important to have safety top but I just told u how that is changed to have.
Crimp tool?? Lol!!
A butter knife bending around with pressure pushing on tip with finger no one can tell. I have other things I made as easier cheap crimp tool.

Hope this helped u.

Sent from my SAMSUNG-SM-G890A using Tapatalk

Holy shit that is epic skills there.

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Originally Posted by jolter604

Holy shit that is epic skills there.

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Not my invention, found it searching Web years ago and tried it!!
Being mechanically minded I can follow the technique and even modify.
But someone thought this out.
I have springs in compression type vice I have set up too.
Like the post with wooden deal he made.
Use something to assist....

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